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Armoloy Specifications

ASTM B568

Standard Test Method for Measurement of Coating Thickness by X-Ray Spectrometry

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Armoloy Specifications

What is ASTM B568?

ASTM B568 is a widely recognized standard developed by ASTM International for the non-destructive measurement of coating thickness using X-ray spectrometry. This method is primarily used for analyzing single-layer and multilayer metallic coatings applied to various substrates.

The standard outlines how X-ray fluorescence (XRF) or X-ray emission techniques can be used to determine coating thickness quickly, accurately, and without damaging the sample. It is especially useful in quality assurance, process control, and research applications where coating precision is critical.

ASTM B568 applies to coatings such as chromium, nickel, gold, silver, zinc, tin, and cadmium.

The test is valuable when coatings are used for corrosion protection, conductivity, solderability, or aesthetic finishes, and must be applied within tight tolerance ranges.

Part ready for X-ray inspection per ASTM B568

The Role of ASTM B568 in Chromium and Nickel Coatings

Chromium Coatings

Chromium coatings—including thin dense chrome and decorative chrome—require precise thickness control to balance hardness, wear resistance, and corrosion protection. ASTM B568 enables in-process and final inspection measurements that ensure uniform coverage without exceeding tolerance limits that could lead to brittleness or dimensional change.

It is particularly important in aerospace, injection molding, and fluid handling components where tight dimensional control is essential.

Nickel Coatings

Nickel coatings—especially electroless nickel and electrolytic nickel—are often used for their corrosion resistance and dimensional stability. ASTM B568 allows for:

  • Measuring deposit thickness over complex geometries
  • Verifying multilayer builds (e.g., chromium over nickel)
  • Ensuring uniform plating in electronics and precision components

Because nickel coatings often require specification to the micron or sub-micron level, X-ray-based measurement provides an efficient, lab-grade solution to validate production standards.

X-ray spectrometer machine for ASTM B568 measurement of coating thickness

ASTM B568 Testing Methodology & Results

The method relies on X-ray fluorescence spectrometry, a technique in which a beam of X-rays is directed at the coated sample. This causes atoms in the coating to emit secondary X-rays (fluorescence), which are detected and analyzed to determine the elemental composition and thickness of the coating.

How It Works:

  1. A known-energy X-ray source excites atoms in the coating
  2. The sample emits characteristic X-rays, which are captured by a detector
  3. The intensity of the detected signal correlates with coating thickness based on pre-calibrated standards

Key Parameters:

  • Elemental composition of both coating and substrate must be known
  • Calibration curves or standard reference materials (SRMs) are used for accuracy
  • Can measure layers as thin as a few nanometers and as thick as hundreds of microns
  • Works best for flat or slightly curved surfaces and metallic layers

Types of Coatings Measured:

  • Single-layer coatings (e.g., nickel on steel)
  • Multilayer coatings (e.g., gold over nickel over copper)
  • Alloyed coatings (e.g., electroless nickel-phosphorus)
astm and ams values around magnifying glass

Industries that Use ASTM B568

  • Aerospace: Used to validate thickness of critical wear-resistant or anti-corrosion coatings on turbine blades, landing gear, and fasteners—especially when tight tolerances matter.
  • Automotive: Measures plating on fuel injectors, pistons, and connectors for performance and longevity.
  • Medical Devices: Non-destructive evaluation is critical for implantable and surgical tools that require biocompatible coatings like BIO-TDC or ME-92.
  • Oil and Gas: Ensures protective coatings (like nickel-phosphorus) are applied to downhole components or valves to withstand corrosive environments.
  • Semiconductors: Essential for gold, silver, and nickel coatings on circuit boards, connectors, and microchips, where layers may be only microns thick.
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Benefits of Working with an ASTM B568 Provider

Non-destructive testing

Unlike destructive cross-sectioning or weight-loss methods, ASTM B568 allows inspection without sacrificing a part—ideal for high-value or limited-quantity components

Micron-level accuracy

Enables tight process control over coating deposition, ensuring performance standards are met across batches and geometries

Faster quality control

Results are available in seconds, speeding up manufacturing timelines and reducing downtime for QA approval

Multilayer analysis

ASTM B568 can detect and measure multiple coatings in sequence, especially useful for complex finishes in electronics or decorative applications

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Specifications at Armoloy

Armoloy offers plating solutions that meet ASTM B568 to support both regulatory compliance and individual project needs. Explore common specifications and accreditations we work with and contact us to find the right solution for your application.